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  • Product Name:   N-(9-Fluorenylmethoxycarbonyloxy)succinimide
  • Synonyms:   1-[[(9h-fluoren-9-ylmethoxy)carbonyl]oxy]-5-pyrrolidinedione;9-fluorenylmethoxycarbonyloxysuccinimide;CARBONIC ACID 2,5-DIOXO-PYRROLIDIN-1-YL ESTER 9H-FLUOREN-9-YLMETHYL ESTER;CARBONIC ACID FLUORENYLMETHYL SUCCIN-N-YL-ESTER;FMOC-OSU
  • CAS No.:   82911-69-1
  • Molecular Formula:   C19H15NO5
  • Molecular Weight :   337.33
  • Specification :   98%
  • Place of Origin:   China
  • Appearance :   
  • Document :   Download

Description of N-(9-Fluorenylmethoxycarbonyloxy)succinimide



N-(9-Fluorenylmethoxycarbonyloxy)succinimide Chemical Properties


Melting point  150-153 °C(lit.)


Boiling point  150-153°C


density  1.3460 (rough estimate)


refractive index  1.5000 (estimate)


storage temp.  2-8°C


solubility  Soluble in dimethyl sulfoxide and dimethyl formamide.


form  Microfine Powder


color  White or almost white


Sensitive  Moisture Sensitive


BRN  3569540


CAS DataBase Reference 82911-69-1(CAS DataBase Reference)




Safety Information


Hazard Codes  Xi,N,Xn


Risk Statements  36/37/38-51/53-43-22


Safety Statements  22-24/25-26/37/39-26-61-37-24


RIDADR  UN 3077 9 / PGIII


WGK Germany  3


10-21


Hazard Note  Moisture Sensitive


HazardClass  9


HS Code  29251995




N-(9-Fluorenylmethoxycarbonyloxy)succinimide Usage And Synthesis


Chemical Properties White powder


Uses Used in conjunction with Isothiocyanate to conduct partial Edman Degradation on biologically active peptides.


Uses N-protecting reagent for oligonucleotide and peptide syntheses


Uses Reagent for the preparation of pure Fmoc amino acids free from contamination by Fmoc-dipeptides.


Purification Methods Recrystallise the carbonate from CHCl3/Et2O, or from pet ether (b 40-60o). [Pauet Can J Chem 60 976 1982, Lapatsaris et al. Synthesis 671 1983.]




N-(9-Fluorenylmethoxycarbonyloxy)succinimide Preparation Products And Raw materials


Preparation Products [2-[2-(Fmoc-amino)ethoxy]ethoxy]acetic acid


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