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  • Product Name:   [Bis(trifluoroacetoxy)iodo]benzene
  • Synonyms:   PIFA ;BTI~Iodosobenzene bis(trifluoroacetate)~Phenyliodine(III) bis(trifluoroacetate)~PIFA;phenylbis(trifluoroacetato-O)iodine;Bis-Trifluoroacetoxyiodobenzene99%;Bis-Trifluoroacetoxyiodobenzene 99%
  • CAS No.:   2712-78-9
  • Molecular Formula:   C10H5F6IO4
  • Molecular Weight :   430.04
  • Specification :   98%
  • Place of Origin:   China
  • Appearance :   
  • Document :   Download

Description of [Bis(trifluoroacetoxy)iodo]benzene
[Bis(trifluoroacetoxy)iodo]benzene Chemical Properties
Melting point  121-125 °C(lit.)
storage temp.  Keep Cold
form  Crystalline Powder
color  White to pale yellow
Water Solubility  insoluble
Sensitive  Moisture & Light Sensitive
BRN  764767
CAS DataBase Reference 2712-78-9(CAS DataBase Reference)
Safety Information
Hazard Codes  Xi
Risk Statements  36/37/38
Safety Statements  26-36-37/39
WGK Germany  3
F  4.10-8-9-21
Hazard Note  Irritant/Keep Cold
HazardClass  IRRITANT, KEEP COLD, LIGHT SENSITIVE
HS Code  29036990
[Bis(trifluoroacetoxy)iodo]benzene Usage And Synthesis
Chemical Properties White to pale yellow crystalline powder
Uses In oxidation, cyclization, dehydrogenation, and dearomatization reactions.
Purification Methods Crystallise the iodo compound from warm trifluoroacetic acid and dry it over NaOH pellets. Recrystallise it also from Me2CO/pet ether. Its melting point depends on the heating rate. [Spyroudis & Varvoglis Synthesis 445 1975, application: Almond et al. Org Synth 66 132 1988.]
[Bis(trifluoroacetoxy)iodo]benzene Preparation Products And Raw materials
Raw materials Dichloromethane-->Hexane-->Hydrogen peroxide-->Trifluoroacetic anhydride-->Sodium percarbonate-->Iodobenzene

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